Process Gas Chromatographs Fundamentals Design and Implementation 1st Edition by Tony Waters ISBN 9781119633013 111963301X
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ISBN 10: 111963301X
ISBN 13: 9781119633013
Author: Tony Waters
Process Gas Chromatographs Fundamentals Design and Implementation 1st Edition Table of contents:
Part One: PGC fundamentals
1 An introduction
Chromatographic separation
The gas chromatograph
The oven
The sample injection valve
The column
The detector
Did you get it?
Self‐assessment quiz: SAQ 01
Student evaluation test: SET 01
References
Figures
New technical terms
2 Peak shape
How columns work
How peaks form
Some conclusions
Did you get it?
Self‐assessment quiz: SAQ 02
Student evaluation test: SET 02
References
Figures
Equation
Symbols
New technical terms
3 Separation
How peaks get separated
Measurements from chromatograms
Did you get it?
Self‐assessment quiz: SAQ 03
Student evaluation test: SET 03
References
Figures
Equations
Symbols
New technical terms
4 Peak patterns
Predictable patterns in peak position
Predictable patterns in peak width
Predictable patterns in retention
Did you get it?
Self‐assessment quiz: SAQ 04
Student evaluation test: SET 04
References
Figures
Equations
Symbols
New technical terms
Part Two: PGC analytics
5 Industrial gas chromatographs
Process analyzers
Process gas chromatographs
Competing technologies
The PGC analytics unit
Did you get it?
Self‐assessment quiz: SAQ 05
Student evaluation test: SET 05
References
Figures
Table
Symbol
New technical terms
6 Carrier gas system
Choice of carrier gas
Carrier gas purity
Carrier gas supply system
Pressure regulation
Flow regulation
Did you get it?
Self‐assessment quiz: SAQ 06
Student evaluation test: SET 06
References
Table
Figures
Symbols
New technical terms
7 Sample injection
Introduction
Injecting gas samples
Injecting liquid samples
Other techniques
Did you get it?
Self‐assessment quiz: SAQ 07
Student evaluation test: SET 07
References
Tables
Figures
Symbols
New technical terms
8 Chromatographic valves
Valve technology
The strange effect of competition
Valve types
Valve leaks
Valve leak mitigation
Did you get it?
Self‐assessment quiz: SAQ 08
Student evaluation test: SET 08
References
Table
Figures
New technical terms
9 Column systems
Two fundamental issues
The temperature ramp solution
The multiple column solution
The choice
Delayed injection
Four types of column system
Type A: A single column
Type B: Multiple columns, single detector
Type C: Multiple detectors, single injector
Type D: Multiple sample injectors
Elemental column systems
Backflush column system
Distribution column system
Heartcut column system
The real power
Endnote
Did you get it?
Self‐assessment quiz: SAQ 09
Student evaluation test: SET 09
References
Table
Figures
New technical terms
10 Detectors
Introduction
Types of detector
Thermal conductivity detector
Flame ionization detector
Flame photometric detector
Other detectors
Did you get it?
Self‐assessment quiz: SAQ 10
Student evaluation test: SET 10
References
Tables
Figures
Equations
Symbols
New technical terms
11 Temperature control
Need for stability
The air‐bath oven
The airless oven
Direct column heating
PGC standardization
A closing thought
Did you get it?
Self‐assessment quiz: SAQ 11
Student evaluation test: SET 11
References
Table
Figures
New technical terms
Part Three: PGC control
12 Event scheduling
A sequence of actions
Timing mechanisms
Control of analyzer operation
Peak identification
Did you get it?
Self‐assessment quiz: SAQ 12
Student evaluation test: SET 12
References
Figures
New technical terms
13 Data display techniques
The chromatogram display
The bargraph display
The trend record
Digital signal processing
PGC function alarms
Did you get it?
Self‐assessment quiz: SAQ13
Student evaluation questions: SET‐13
References
Table
Figures
New technical terms
14 Peak area integration
Digital chromatogram processing
Quantifying the analyte peaks
Measuring overlapping peaks
Did you get it?
Self‐assessment quiz: SAQ 14
Student evaluation test: SET 14
References
Figures
New technical terms
15 Calibration
Measurement principles
Calibration methods
Did you get it?
Self‐assessment quiz: SAQ 15
Student evaluation test: SET 15
References
Figure
Equations
Symbols
New technical terms
Answers to self‐assessment questions
BibliographyBibliography
Glossary
Index
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