Analytical Characterization Methods for Crude Oil and Related Products 1st Edition by Ashutosh Shukla ISBN 1119286318 9781119286318

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Product details:

ISBN 10:      1119286318
ISBN 13: 978-1119286318
Author:      Ashutosh K. Shukla

Basic theory, applications, and recent trends in analytical techniques used in crude oil and related products analysis

This book covers the application of different spectroscopic methods to characterize crude oil and related products. Its topics are presented in a pedagogical manner so that those new to the subject can better understand the content. The book begins by familiarizing the reader with the rheological characterization of crude oil and related products. Subsequent chapters are directed towards the current trends of different spectroscopic methods for the characterization of crude oil.

Analytical Characterization Methods for Crude Oil and Related Products features chapters on: optical interrogation of petroleum asphaltenes (myths and reality); ESR characterization of organic free radicals in petroleum products; high-field, pulsed, and double resonance studies of crude oils and their derivatives; NMR spectroscopy in bitumen characterization; applications of Raman spectroscopy in crude oil and bitumen characterization; and more. 

• Uses a bottom-up approach―starting from the basic theory of the technique followed by its applications and recent trends in crude oil analysis
• Includes informative content so as to take a technician to the level of using a particular analytical method
• Covers relevany information so as to enable a manager in the industry to make purchasing decisions

Analytical Characterization Methods for Crude Oil and Related Products is aimed at researchers in academia as well as technicians and developers of new analytical methods in the oil industry and related areas. It will also be of interest to professionals, scientists, and graduate students in analytical sciences dealing with oil and environmental analysis. 

Analytical Characterization Methods for Crude Oil and Related Products 1st  Table of contents:

 

Chapter 1: Rheological Characterization of Crude Oil and Related Products
1.1 Introduction
1.2 Sample Preparation for Rheological Characterization
1.3 Rheological Tests
1.4 Potential Sources of Errors
References

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Chapter 2: Optical Interrogation of Petroleum Asphaltenes: Myths and Reality
2.1 Introduction
2.2 Mythical “Characteristic Signatures” of Asphaltenes in Optical Analytical Methods
2.3 Misconceptions about the Properties of UV/Vis Absorption Spectra of Asphaltenes
2.4 Current State of Knowledge about Asphaltene Monomers and Primary Asphaltene Aggregates
References

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Chapter 3: ESR Characterization of Organic Free Radicals in Crude Oil and By-Products
3.1 Introduction
3.2 Organic-Free Radicals in Crude Oil
3.3 ESR of Crude Oil
3.4 By-Product Oil by ESR
3.5 ESR and Calculations on the Electronic Structure of Free Radicals in Oil By-Products
References

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Chapter 4: High-Field, Pulsed, and Double Resonance Studies of Crude Oils and their Derivatives
4.1 Introduction
4.2 EPR: Basic Principles and Magnetic Interactions
4.3 EPR Pulse Sequences
4.4 Application Examples
4.5 Conclusion
Acknowledgments
References

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Chapter 5: NMR Spectroscopic Analysis in Characterization of Crude Oil and Related Products
5.1 Introduction
5.2 1H NMR and 13C NMR Spectroscopy Analysis Methods
5.3 NMR Techniques
5.4 Application of NMR Analysis in Characterization of Crude Oil and Related Products
5.5 Asphaltene Characterization using NMR Techniques
5.6 Conclusions
References

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Chapter 6: NMR Spectroscopy in Bitumen Characterization
6.1 Introduction
6.2 1H and 13C NMR Spectroscopy
6.3 Phosphorus-31 NMR Spectroscopy
6.4 NMR Imaging and Solid-State NMR
6.5 Conclusion
References

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Chapter 7: Applications of Low Field Magnetic Resonance in Viscous Crude Oil/Water Property Determination
7.1 Introduction
7.2 Background for NMR Measurements
7.3 Fluid Content in Oil/Water Systems
7.4 Oil Viscosity from NMR
7.5 Fluid Saturations and Viscosity in Porous Media
7.6 NMR in Oil-Solvent Systems
7.7 Summary of NMR and Fluid Property Measurements
Acknowledgments
References

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Chapter 8: Application of Near-Infrared Spectroscopy to the Characterization of Petroleum
8.1 Introduction
8.2 Sample Handling and Preparation
8.3 Near-Infrared Spectroscopy
8.4 Chemometrics
8.5 Commercial NIR Equipment and Industrial Applications
8.6 Conclusions
References

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Chapter 9: Raman and Infrared Spectroscopy of Crude Oil and its Constituents
9.1 Introduction
9.2 Fundamentals of Raman and Infrared Spectroscopy
9.3 Infrared Spectroscopy
9.4 Raman Spectroscopy
9.5 Evaluation of Vibrational Spectra
9.6 Applications
9.7 Conclusion

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