Fluorous Chemistry 1st by Gladysz 352730617X 9783527306176

Fluorous Chemistry 1st by John A. Gladysz – Ebook Instant Download/Delivery ISBN:352730617X , 9783527306176

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Table of contents:

Fluorous chemistry : scope and definition / Istvan T. Horvath, Dennis P. Curran and J. A. Gladysz

A personal view of the history of fluorous chemistry / Istvan T. Horvath

Fluorous solvents and related media / J. A. Gladysz and Charlotte Emnet

Strategies for the recovery of fluorous catalysts and reagents : design and evaluation / J. A. Gladysz and Rosenildo Correa da Costa

Ponytails : structural and electronic considerations / J. A. Gladysz

Partition coefficients involving fluorous solvents / J. A. Gladysz, Charlotte Emnet and Jozsef Rabai

Separations with fluorous silica gel and related materials / Dennis P. Curran

Light fluorous chemistry – a user’s guide / Dennis P. Curran

Getting started in synthesis : a tabular guide to selected monofunctional fluorous compounds / Jozsef Rabai

Synthetic applications of fluorous reagents / Sivaraman Dandapani

Radical carbonylations using fluorous tin reagents : convenient workup and facile recycle of the reagents / Ilhyong Ryu

Approaches to the fluorous Mitsunobu reaction / Roman Dembinski

Recyclable oxidation reagents / David Crich and Yekui Zou

Fluorous protecting groups and tags / Wei Zhang

Fluorous scavengers / Craig W. Lindsley and William H. Leister

Synthesis of perfluoroalkylated phosphines / Eric G. Hope and Alison M. Stuart

Metal catalyzed carbon – carbon bond forming reactions in fluorous biphasic systems / Siegfried Schneider, Carl Christoph Tzschucke and Willi Bannwarth

Hydroformylation and hydrogenation catalyzed by perfluoroalkylated phosphine/metal complexes / Eric G. Hope and Alison M. Stuart

Hydroformylation catalyzed by rhodium/fluorinated triarylphosphite complexes in fluorous biphasic media / Eric Monflier, Andre Mortreux and Yves Castanet

Fluorous nitrogen ligands for oxidation reactions / Gianluco Pozzi and Silvio Quici

Synthesis of fluorous nitrogen ligands and their metal complexes as precatalysts for applications in alkane, alkene, and alcohol oxidation, and atom transfer radical reactions / Jean-Marc Vincent, Dominique Lastecoueres, Maria Contal, Mariano Laguna and Richard H. Fish

Enantioselective catalysis : biphasic conditions / Denis Sinou

Enantioselective catalysis in non-biphasic conditions / Seiji Takeuchi and Yutaka Nakamura

Combining lipase-catalyzed knietic resolutions of racemic alcohols with fluorous phase labeling / Fritz Theil, Helmut Sonnenschein, Benno Hungerhoff and Sauda M. Swaleh

Enantiomeric partitioning using fluorous biphase methodology in lipase-mediated (trans)esterifications / Petr Beier and David O’Hagan

Selective and clean reactions in fluorinated alcohols / Jean-Pierre Begue, Daniele Bonnet-Delpon and Benoit Crousse

Liquid/solid catalyst-recycling method without fluorous solvents / Kazuaki Ishihara and Hisashi Yamamoto

Microwave-assisted fluorous chemistry / Kristofer Olofsson and Mats Larhed

(R)-6,6′-diperfluorobutyl-1,1′-binaphthyl-2,2′-diol : the copper-mediated perfluorobutylation of dibromobinaphthol / Kin Shing Chan and Yuan Tian

(R)- and (S)-4,4’6,6′-tetraperfluorooctyl-1,1′-binaphthyl-2,2′-diol : the copper-mediated perfluorooctylation of tetrabromobinaphthol and resolution / Kin Shing Chan and Yuan Tian

4-aminobenzoic acid : the Staudinger reduction with a fluorous phosphine reagent / Craig W. Lindsley and Zhijian Zhao

1,2-diethyl-6a, 10-dimethoxy-1,6a, 11b, 11c-tetrahydro-2H-benzo(kl)xanthen-4-one, [beta],[beta]-phenolic coupling reactions to access unnatural carpanone analogs with a fluorous diacetoxy iodobenzene (F-DAIB) reagent / Craig W. Lindsley and Zhijian Zhao

4-nitro-1,1′-biphenyl : Suzuki coupling in liquid/liquid FBS / C. Christoph Tzschucks, Siegfried Schneider and Willi Bannwarth

1-(4-nitrophenyl)-2-phenylacetylene : Sonogashira coupling in liquid/liquid FBS / C. Christoph Tzschucke, Siegfried Schneider and Willi Bannwarth

4-nitro-1,1′-biphenyl : Suzuki coupling with a catalyst on FRPSG without a perfluorinated solvent / C. Christoph Tzchucke, Siegfried Schneider and Willi Bannwarth

1-(4-nitrophenyl)-2-phenylacetylene : Sonogashira coupling with a catalyst on FRPSG without a perfluorniated solvent / C. Christoph Tschucke, Siegfried Schneider and Willi Bannwarth

Tris(4-perfluorohexylphenyl)phosphine : synthesis of perfluoroalkyl arylphosphines by copper-mediated cross coupling / Weiping Chen and Jianliang Xiao

Tris[4-(1H,1H,2H,2H-perfluorooctyl)phenyl]phosphine : synthesis of fluoroalkyl arylphosphines by the Heck reaction / Weiping Chen and Jianliang Xiao

3,5-bis(perfluorodecyl)phenylboronic acid : an easily recyclable direct amide condensation catalyst / Kazuaki Ishihara and Hisashi Yamamato

Fluorous-tagged tetrafluorophenylbis(triflyl)methane : an organic solvent-swellable and strong Bronsted acid catalyst / Kazuaki Ishihara and Hisashi Yamamoto

Tetrakis[[mu]-3,5-bis(perfluorooctyl)benzoato-O,O’] dirhodium : application as a recyclable catalyst for a carbenoid cyclopropanation reaction / Gerhard Maas and Andreas Endres

1,4,7-tris-N-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)-1,4,7-triazacyclononane [R[subscript f]-TACN] : a fluorous soluble nitrogen ligand via alkylation with a fluoroponytail, C₈F₁₇(CH₂)₃I / Jean-Marc Vincent and Richard H. Fish

Mn[superscript 2+]/CO[superscript 2+]/Cu[superscript 2+]/Cu[superscript +] complexes of fluoroponytailed R[subscript f]-tris-n-1,4,7-triazacyclononane and R[subscript f]-carboxylate, C₈F₁₇(CH₂)₂COOH : precatalysts for FBC alkane, alkene, and alcohol oxidation chemistry / Jean-Marc Vincent, Maria Contel, Mariano Laguna and Richard H. Fish

6,6,7,7,8,8,9,9,10,10,11,11,12,12,13,13,13-heptadecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)tridecanoic acid (bis-R[subscript f]-carboxylate), [C₈F₁₇(CH₂)₃]₂CHCOOH : a fluorous soluble carboxylic acid ligand for metal complexes / Jean-Marc Vincent and Richard H. Fish

1H,1H,2H,2H-heptadecafluorodecyl nicotinate (1) and bis(1H,1H,2H,2H-heptadecafluorodecyl)pyridine-3,5-dicarboxylate (2) : esterification of nicotinic acid with a fluoroalcohol / Takahiro Nishimura and Sakae Uemura

Pyridine-3-carbaldehyde bis(1H,1H,2H,2H-heptadecafluorodecyl) acetal : acetalization of pyridine-3-carbaldehyde with a fluoroalcohol / Takahiro Nishimura and Sakae Uemura

2,2,2-trifluoroethyl 2H,2H,3H,3H-perfluoroundecanoate : a highly fluorinated acyl donor useful for the lipase catalyzed labeling of racemic alcohols [1] / Fritz Theil, Helmut Sonnenschein, Benno Hungerhoff and Sauda M. Swaleh

(R)- and (S)-1-phenylethanol : kinetic resolution of the racemic alcohol by lipase catalyzed enantiomer-selective fluorous phase labeling / Fritz Theil, Helmut Sonnenschein, Benno Hungerhoff and Sauda M. Swaleh

(R)- and (S)-1-naphthalen-2-yl-ethanol : kinetic resolution of the racemic alcohol by lipase catalyzed enantiomer-selective fluorous phase delabeling of a corresponding highly fluorinated ester / Fritz Theil, Helmut Sonnenschein, Benno Hungerhoff and Sauda M. Swaleh

Tris[4-(1H,1H-pentadecafluorooctyloxy)phenyl]phosphane / Dennis Sinou and David Maillard

Bis(1H,1H,2H,2H-perfluorooctyl) tin oxide and 1,3-dichlorotetra(1H,1H,2H,2H-perfluorooctyl)distannoxane : synthesis and applications of fluorous distannoxanes / Junzo Otera

Gb3 oligosaccharide derivative : fluorous synthesis of an oligosaccharide / Tsuyoshi Miura and Toshiyuki Inazu

Thyrotropin-releasing hormone [1] (TRH) : peptide synthesis on a fluorous support / Mamoru Mizuno, Kohtaro Goto, Tsuyoshi Miura and Toshiyuki Inazu

Perfluorooctylpropyl alcohol : radical addition of perfluorooctyl iodide to triallyl borate, followed by reductive dehalogenation and aqueous deprotection / Jozsef Rabai, Istvan Kovesi and Ana-Maria Bonto

Perfluorooctylpropyl amine : use of perfluorooctylpropyl iodide for a Gabriel synthesis of a fluorophilic amine / Jozsef Rabai, Abudurexiti Abulikemu and Denes Szabo

Cyclohexyl acetate : the acylation reaction with a fluorous lanthanide catalyst in supercritical carbon dioxide with or without a fluorous solvent / Koichi Mikami, Hiroshi Matsuzawa, Joji Nishikido and Mayumi Kamishima

p-methoxyacetophenone : the Friedel-Crafts acylation with a fluorous lanthanide catalyst / Koichi Mikami, Hiroshi Matsuzawa and Joji Nishikido

Tris(4-tridecafluorohexylphenyl)phosphine : versatile ligand synthesized via copper catalyzed cross coupling with a perfluoroalkyl iodide, lithiation and condensation reactions / Dave J. Adams, Eric G. Hope, Alison M. Stuart and Andrew J. West

(R)-6,6′-bis(tridecafluoro-n-hexyl)-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl((R)-Rf-BINAP) : a multi-step sequence to a chiral perfluoroalkylated bidentate phosphine ligand / Dave J. Adams, Eric G. Hope, Alison M. Stuart and Andrew J. West

4-fluorobenzyl 4-(4-nitrophenyl)butyrate : the Mitsunobu reaction with a fluorous phosphine and a fluorous dead reagent / Dennis P. Curran and Sivaraman Dandapani

(R)-6,6′-bis[tris(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)silyl]-1,1′-binaphthalene-2,2′-diol and (R)-6,6′-bis[tris(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)silyl]-2,2′-bis(diphenylphosphino)-1,1′-binaphthalene / Seiji Takeuchi and Yutaka Nakamura

5[alpha]-cholestan-3[alpha]-ol : inversion of configuration via the Mitsunobu reaction with a fluorous gallic acid / Roman Dembinski and Marcin W. Markowicz

1,3-bis(heptadecafluorooctyl)-5-chlorobenzene : synthesis of perfluoroalkylarenes from aryl bromides / Gianluca Pozzi, Marco Cavazzini and Ian Shepperson

3-tert-butyl-5-heptadecafluorooctyl-2-hydroxybenzaldehyde : synthesis of perfluoroalkylarenes from aryl bromides / Gianluca Pozzi, Marco Cavazzini and Ian Shepperson

2-phenyl-4-{[(tris(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)silyl]methyl}-1,3,2-dioxaborolane : the immobilization of boronic acids with a fluorous diol / Feng-Ling Qing

Ytterbium(III) tris(trifluoromethylsulfonyl)methide : preparation of a highly active lanthanide catalyst / Anthony G. M. Barrett, D. Christopher Braddock and Jerome J. P. Peyralans

Bis(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)cyclopenta-1,3-diene : preparation from cyclopenta-1,3-diene : 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-8-iodooctane and 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl triflate / Tomas Briza, Jaroslav Kvicala and Oldrich Paleta

5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluorodec-l-yne : preparation from ethynyldimethylphenylsilane and 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl triflate / Jaroslav Kvicala, Tomas Briza and Oldrich Paleta

N,N’-bis(1H,1H,2H,2H-perfluorooctyl)carbodiimide / Claudio Palomo, Jesus M. Aizpurua and Iraida Loinaz

tert-butoxycarbonyl-[alpha]-aminoisobutyryl-[alpha]-aminoisobutyric acid benzyl ester (Boc-Aib-Aib-OBn) : peptide synthesis with a fluorous carbodiimide reagent / Claudio Palomo, Jesus M. Aizpurua and Iraida Loinaz

N-methyl-N-[1-(20-oxopregna-3,5-dien-3-yl)vinyl]acetamide : regioselective heck coupling reactions with a fluorous tagged bidentate ligand to make 2-acylamino-1,3-butadienes / Karl S. A. Vallin

10-iodo-9H,9H,10H,11H,11H-perfluorononadecane : free radical chain reactions of fluorous primary alkyl iodides / Marc Wende and J. A. Gladysz

Tris(1,1,1,5,5,5-hexafluoroacetylacetonate)chromium(III) : crystallization of a highly fluorinated compound from a CO₂-expanded liquid solvent / Philip G. Jessop, Christopher D. Ablan, Charles A. Eckert and Charles L. Liotta

trans-1,2-dibromocyclohexane : the phase vanishing bromination with FC-72 as a screen phase / Ilhyong Ryu, Hiroshi Matsubara, Hirayuki Nakamura and Dennis P. Curran

1-hydroxymethyladamantane : radical hydroxymethylation with a fluorous tin hydride / Ilhyong Ryu, Hiroshi Matsubara and Dennis P. Curran

5,5-bis(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-2-(4-formylphenyl)-1,3-dioxane : selective acetal formation with fluorous 1,3-diol reagents and its use in multistep synthesis / Roger W. Read and Chutian Zhang

1-(4-methoxyphenoxy)-3-(4-pyridin-2-yl-piperazin-1-yl)-propan-2-ol : the amination reaction using a fluorous isatoic anhydride scavenger to remove excess amine / Wei Zhang and Christine Hiu-Tung Chen

Borane-(1H,1H,2H,2H-perfluorodecyl) methyl sulfide adduct : preparation of a borane-fluorous dialkyl sulfide and its application to the hydroboration of [beta]-pinene / David Crich, Mitesh Patel and Santhosh Neelamkavil

Basic principles and recent advances in fluorinated self-assemblies and colloidal systems / Marie Pierre Krafft

Fluorous nanoparticles / Marcial Moreno-Manas and Roser Pleixats

Self-assembly of hybrid fluorous materials / Pierangelo Metrangolo, Tullio Pilati and Giuseppe Resnati

Fluorous materials for biomedical uses / Jean G. Riess

Fun and games with fluorous chemistry / Jozsef Rabai.

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