Macroscale and Microscale Organic Experiments 7th Edition by Kenneth L Williamson, Katherine M Masters ISBN 1305577191 978-1305577190

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ISBN 10: 1305577191 

ISBN 13: 978-1305577190

Author: Kenneth L. Williamson, Katherine M. Masters

 Succeed in your organic laboratory course with MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS, Seventh Edition. This proven, authoritative manual emphasizes safety and features new themed Modules experiments with real world applications. Using the manual’s mix of macroscale and microscale experiments, you’ll gain the knowledge and confidence you need to perform a wide variety of experiments, as well as experience working with conventionally-sized glassware.

Table of contents: 

1. Introduction

2. Laboratory Safety, Courtesy, and Waste Disposal

3. Melting Points and Boiling Points

4. Recrystallization

5. Distillation

6. Steam Distillation, Vacuum Distillation, and Sublimation

7. Extraction

8. Thin-Layer Chromatography: Analyzing Analgesics and Isolating Lycopene from Tomato Paste

9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments

10. Gas Chromatography: Analyzing Alkene Isomers

11. Infrared Spectroscopy

12. Nuclear Magnetic Resonance Spectroscopy

13. Mass Spectrometry

14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis

15. Computational Chemistry

16. The SN2 Reaction: 1-Bromobutane

17. Nucleophilic Substitution Reactions of Alkyl Halides

18. Radical Initiated Chlorination of 1-Chlorobutane

19. Alkenes from Alcohols: Cyclohexene from Cyclohexanol

20. Bromination and Debromination: Purification of Cholesterol

21. Dichlorocarbene

22. Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid

23. The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent

24. Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-Octadiyn-2,7-Diol

25. Catalytic Hydrogenation

26. Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis

27. Epoxidation of Cholesterol

28. Nitration of Methyl Benzoate

29. Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry

30. Alkylation of Mesitylene

31. The Friedel-Crafts Reaction: Anthraquinone and Anthracene

32. Friedel-Crafts Acylation of Ferrocene: Acetylferrocene

33. Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical

34. 1,2,3,4-Tetraphenyl-Naphthalene via Benzyne

35. Triptycene via Benzyne

36. Aldehydes and Ketones

37. Dibenzalacetone by the Aldol Condensation

38. Grignard Synthesis of Triphenylmethanol and Benzoic Acid

39. The Wittig and Wittig-Horner Reactions

40. Esterification and Hydrolysis

41. Acetylsalicylic Acid (Aspirin)

42. Malonic Ester of a Barbiturate

43. Amines

44. The Sandmeyer Reaction: 1-Bromo-4-Chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene

45. Synthesis and Bioassay of Sulfanilamide and Derivatives

46. Dyes and Dyeing

47. Martius Yellow

48. Diels-Alder Reaction

49. Ferrocene [Bis(Cyclopentadienyl)Iron]

50. A Diels-Alder Reaction Puzzle: The Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride

51. Tetraphenylcyclopentadienone

52. Hexaphenylbenzene and Dimethyl Tetraphenylphthalate

53. The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine

54. Nitric Acid Oxidation; Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline

55. The Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil

56. The Synthesis of 2,2-Dimethyl-1,5-Dioxolane; The Acetonide Derivative of a Vicinal Diol

57. 1,4-Addition: Reductive Acetylation of Benzil

58. The Synthesis of an Alkyne from an Alkene by Bromination and Dehydrobromination: Stilbene and Diphenylacetylene

59. The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid and Its Decarboxylation to cis-Stilbene

60. Multicomponent Reactions: The Aqueous Passerini Reaction

61. Chemiluminescence: Syntheses of Cyalume and Luminol

62. Photochemistry: The Synthesis of Benzopinacol

63. Carbohydrates and Sweeteners

64. Virstatin, a Possible Treatment for Cholera

65. Biosynthesis of Ethanol and Enzymatic Reactions

66. The Synthesis of Natural Products: The Sex Attractant of the Cockroach and Camphor

67. Polymers: Synthesis and Recycling

68. Searching the Chemical Literature

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Tags: Kenneth L Williamson, Katherine M Masters, Macroscale, Microscale, Organic Experiments