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Modern Sample Preparation for Chromatography 2nd Edition by Serban Moldoveanu, Victor David ISBN 0323898203 970323898201

Name: Modern Sample Preparation for Chromatography 2nd Edition by Serban Moldoveanu, Victor David ISBN 0323898203 970323898201
SKU: EB-27335236
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Modern Sample Preparation for Chromatography 2nd Edition Serban Moldoveanu Victor David Digital Instant Download

Author(s): Serban Moldoveanu Victor David

Edition: 2

File Details: PDF, 12.24 MB

Year: 2021

Language: english

SKU: EB-27335236 Category: Chemistry Tag: Serban Moldoveanu Victor David

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Modern Sample Preparation for Chromatography 2nd Edition by Serban Moldoveanu, Victor David – Ebook PDF Instant Download/Delivery: 0323898203, 978-0323898201
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ISBN 10: 0323898203
ISBN 13: 978-0323898201
Author: Serban Moldoveanu, Victor David

Modern Sample Preparation for Chromatography, Second Edition explains the principles of sample preparation for chromatographic analysis. A variety of procedures are applied to make real-world samples amenable for chromatographic analysis and to improve results. This book’s authors discuss each procedure’s advantages, disadvantages and their applicability to different types of samples, along with their fit for different types of chromatographic analysis. The book contains numerous literature references and examples of sample preparation for different matrices and new sections on green approaches in sample preparation, progress in automation of sample preparation, non-conventional solvents for LLE (ionic liquids, deep eutectic mixtures, and others), and more.

Presents numerous techniques applied for sample preparation for chromatographic analysis
Provides an up-to-date source of information regarding the progress made in sample preparation for chromatography
Describes examples for specific types of matrices, providing a guide for choosing the appropriate sample preparation method for a given analysis

Modern Sample Preparation for Chromatography 2nd Table of contents:

I. General Concepts in Sample Preparation

Chapter 1: Preliminaries to Sample Preparation
1.1. Collection of Information and Planning for Chromatographic Analysis
1.2. Statistical Evaluation of Quantitative Data
1.3. Validation of Analytical Methods
1.4. Sampling

Chapter 2: The Role of Sample Preparation
2.1. Preliminary Processing of the Sample
2.2. Routine Manipulations
2.3. Sample Cleanup and Fractionation
2.4. Concentration of the Sample
2.5. Chemical Modifications
2.6. Selecting Sample Preparation Procedures
2.7. Automation and High-Throughput Preparation

Chapter 3: Chromatography as Core Analytical Procedure
3.1. Basic Concepts in Chromatography
3.2. Gas Chromatography Overview
3.3. High-Performance Liquid Chromatography Overview
3.4. Other Chromatographic Methods

II. Main Sample Preparation Techniques

Chapter 4: Mechanical Processing
4.1. Grinding and Sieving
4.2. Filtration, Microfiltration, and Ultrafiltration
4.3. Centrifugation

Chapter 5: Phase Transfer Techniques
5.1. Distillation and Drying
5.2. Crystallization and Precipitation

Chapter 6: Solvent Extraction
6.1. Properties of Solvents in Extraction
6.2. Conventional Liquid–Liquid Extraction
6.3. Special Liquid–Liquid Extraction
6.4. Conventional Liquid–Solid Extraction
6.5. Accelerated Solvent Extraction
6.6. Microwave and Ultrasound-Assisted Extraction
6.7. Supercritical Solvent Extraction
6.8. Solvent-Gas Extraction

Chapter 7: Solid-Phase Extraction
7.1. Conventional SPE
7.2. Sorbent Materials and Their Characterization
7.3. Types of SPE Sorbents
7.4. SPE Formats
7.5. Retention and Elution Mechanisms
7.6. Solvents in SPE
7.7. SPE Optimization
7.8. Headspace SPE
7.9. Solid-Phase Microextraction
7.10. Stir-Bar Sorptive Extraction
7.11. Matrix Solid-Phase Dispersion
7.12. QuEChERS

Chapter 8: Chromatographic Procedures as Preliminary Separations
8.1. Thin-Layer and Open Column Liquid Chromatography
8.2. Size-Exclusion Chromatography
8.3. Other Chromatographic Techniques

Chapter 9: Membrane Separations
9.1. Gas Diffusion Through Membranes
9.2. Membranes in Liquid–Liquid Extraction
9.3. Reversed Osmosis and Dialysis

Chapter 10: Electroseparations in Sample Preparation
10.1. Electrophoretic Techniques
10.2. Other Electroseparation Techniques

Chapter 11: Other Separation Techniques
11.1. Ion Exchange in Sample Preparation
11.2. Additional Techniques

Chapter 12: The Role of Derivatization
12.1. Derivatization for Sample Dissolution
12.2. Improvement of Gas Chromatography by Derivatization
12.3. Liquid Chromatography Improvements
12.4. Derivatization for Chiral Separations

Chapter 13: Chemical Reactions in Derivatization
13.1. Alkyl or Aryl Derivative Formation
13.2. Silyl Derivative Formation
13.3. Acylation Reactions
13.4. Addition Reactions in Derivatization
13.5. Cyclic Compound Formation
13.6. Other Derivatization Reactions
13.7. Solid-Phase Derivatization

Chapter 14: Chemical Degradation of Polymers
14.1. Chemical Degradation of Carbohydrates
14.2. Degradation of Proteins
14.3. Degradation of Other Macromolecules

Chapter 15: Sample Preparation for Different Materials
15.1. Environmental Analysis (Air, Water, Soil)
15.2. Pharmaceuticals Analysis
15.3. Biological Samples
15.4. Food and Agricultural Products
15.5. Analysis of Other Materials

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