The Wolff Kishner Reduction and Related Reactions Discovery and Development 1st Edition by David Lewis 0128157275 9780128157275

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Product details:

ISBN 10: 0128157275 

ISBN 13: 9780128157275

Author: David E. Lewis 

The Wolff-Kishner Reduction and Related Reactions: Discovery and Development 1st Table of contents:

Chapter 1: The discoverers of the reaction
Abstract
Nikolai Matveevich Kizhner: A truly eventful life 
Ludwig Wolff 
Chapter 2: Discovery and priority
Abstract
1911–1913: Kizhner’s initial disclosures of the reaction
1911: Wolff’s version of the reaction
Settling the question of priority
Chapter 3: Early studies of the reaction
Abstract
Mechanistic investigations
Pyrazolines and N-alkylhydrazones
Side reactions in the Wolff-Kishner reduction
Early exploration of the scope and limitations of the reaction
Higher terpenoids and steroids
Heterocyclic compounds and alkaloids
Chapter 4: The Huang-Minlon modification
Abstract
Introduction
The Huang-Minlon modification of the Wolff-Kishner reduction
Representative applications of the Huang-Minlon method
Limitations of the Wolff-Kishner reduction
A final word…
Chapter 5: Modern adaptations of the Wolff-Kishner reduction
Abstract
Introduction
Effects of steric hindrance on the Wolff-Kishner reaction
Barton and Nagata modifications of the Wolff-Kishner reduction: “Forced” Wolff-Kishner reductions
What about not using a base at all? Deoxygenation by reduction of sulfonylhydrazones
Chapter 6: Kishner reduction-elimination of α-substituted ketones
Abstract
Introduction
Reduction of α-amino-, α-alkoxy- and α-hydroxyketones
The reaction of epoxyketones and 2-acylaziridines with hydrazine: The Wharton and aza-Wharton reactions
The reaction of epoxyketones with tosylhydrazine: The Eschenmoser fragmentation
Chapter 7: Deoxygenation in modern synthesis
Abstract
Introduction
The Huang-Minlon modification
The Barton modification
The Nagata modification
The Wharton and Aza-Wharton reactions
The Eschenmoser fragmentation
The Shapiro reaction

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Tags: The Wolff Kishner, Reduction, Related Reactions, Discovery, Development, David Lewis